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to a chemical examination. Prussian blue is detected by heating with a solution of sodium hydroxide, filtering, acidulating the filtrate with acetic acid, and then adding ferric chloride, when, in its presence, a blue colour will be produced. Indigo is best recognised by the microscopic examination. It is not decolorised by caustic alkali, but it dissolves in sulphuric acid to a blue liquid. Soapstone, gypsum, sand, and metallic iron, are identified by means of the usual chemical reactions. A compound very aptly termed "Lie-tea," is sometimes met with. It forms little pellets, consisting of tea-dust mixed with foreign leaves, sand, etc., and held together by means of gum or starch. This falls to powder if treated with boiling water. In the presence of catechu, the tea infusion usually assumes a muddy appearance upon standing. In case iron salts have been employed to deepen the colour of the infusion, they can be detected by treating the ground tea-leaves with acetic acid, and testing the filtered solution with potassium ferrocyanide. Tea should not turn black upon immersion in hydrosulphuric acid water, nor should it impart a blue colour to ammonia water. The infusion should be ambercoloured, and not become reddened by the addition of an acid.

The United States Tea Adulteration Act was passed by Congress in 1883. The enactment of this law was largely due to the exertions of prominent tea merchants, whose business interests were seriously affected by the sale (principally in trade auctions) of the debased or spurious article. It is stated in the official report of the United States Tea Examiner at New York City, that from March 1883 to December of the same year, 856,281 packages (about four millions of pounds) of tea were inspected, of which 7000 packages (325,000 pounds) were rejected as unfit for consumption. Since the enforcement in New York City of the Tea Adulteration Act, nearly 2000 samples of tea have been chemically tested under the

direction of the author. The proportion grossly adulterated has been a little over nine per cent. But this does not apply to the total amount imported, since only those samples which were somewhat suspicious in appearance were submitted for analysis. As the result of the past two years' experience in the chemical examination of tea, the prevailing adulterations were found to be of two kindsthe admixture of spent tea-leaves, and the application to the tea of a facing preparation. A natural green tea possesses a dull hue, and is but seldom met with in the trade; some Moyunes and uncoloured Japans (which latter, properly speaking, is not a green tea) being almost the only varieties not exhibiting the bright metallic lustre due to the facing process. The addition of foreign leaves was detected only in a few instances; the presence of sand and gravel occurred far more frequently. Apropos of the practical utility of Governmental sanitary legislation, it can be stated that, since the enforcement of the Adulteration Act, the tea imported into the city of New York has very perceptibly improved in quality.

Attempts in tea culture are being made in the United States of Columbia, S.A. A specimen of the prepared plant received by the writer, differed greatly in appearance from the Chinese and Japanese products. The leaves, which had not been rolled but were quite flat, possessed a light pea-green colour and a fine but rather faint aroma. An examination indicated that the tea, although very delicate in quality, was seriously deficient in body. The analysis showed :

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The following Tea Assay, while not including the determinations of all the proximate constituents of the plant, will, it is believed, in most instances suffice to indicate to the analyst the presence of spent leaves, mineral colouring matters, and other inorganic adulterations.

Theine (Caffeine), CH1N,O,.-Contrary to the once general belief, there does not always exist a direct relation between the quality of tea (at least so far as this is indicated by its market price) and the proportion of theine contained, although the physiological value of the plant is doubtless due to the presence of this alkaloid.

The commercial tea-taster is almost entirely guided in his judgment in regard to the value of a sample of tea by the age of the leaf, and by the flavour or bouquet produced upon "drawing," and this latter quality is to be mainly ascribed to the volatile oil.

The following process will serve for the estimation of theine-A weighed quantity of the tea is boiled with distilled water until the filtered infusion ceases to exhibit any colour. The filtrate is evaporated on a water bath to the consistence of a syrup; it is next mixed with calcined magnesia to alkaline reaction, and carefully evaporated to dryness.

The residue obtained is then finely powdered, digested for a day or so with ether (or chloroform) and filtered, the remaining undissolved matter being again digested with a fresh quantity of ether, so long as any further solution of theine takes place. The ether is now removed from the united filtrates by distillation, whereupon the theine will be obtained in a fairly pure condition.

Theine contains a very large proportion of nitrogen (almost 29 per cent.), and Wanklyn* has suggested the application of his ammonia process (see p. 205) to the analysis of tea. Genuine tea is stated to yield from 0.7 to 0.8 per cent of total ammonia, when tested in this manner.

*Tea, Coffee, and Cocoa Analysis.'

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